AnAnolis skin melanophore assay suitable for photoaffinity labeling studies with α-MSH

Summary Visual determination of MSH-induced pigment migration in melanophores of small pieces ofAnolis carolinensis skin is standardized by first measuring photoelectrometrically the change in reflection/transmission of the whole dorsal skin in response to different hormone concentrations. This method allows the rapid and precise recording of time-response curves after photoaffinity labeling of MSH receptors or of dose-response curves of large series of synthetic compounds.Acknowledgments. We wish to thank Ms V. Jäggin, Ms C. Schulthess and Ms G. van Hees for excellent technical assistance, Dr. R. Andreatta, Ciba-Geigy AG, Basel, for his generous gift of -MSH and Prof. A Pletscher for his continuous interest. This work was supported by the Swiss National Science Foundation.     

Bi含量对SrBi4Ti4O15铁电材料性能的影响

~~Bi含量对SrBi_4Ti_4O_(15)铁电材料性能的影响@朱骏$扬州大学物理科学与技术学院!江苏扬州,225002 @毛翔宇$扬州大学物理科学与技术学院!江苏扬州,225002 @卢网平$扬州大学物理科学与技术学院!江苏扬州,225002 @惠荣$扬州大学物理科学与技术学院!江苏扬州,225002 @陆文峰$扬州大学物理科学与技术学院!江苏扬州,225002 @陈小兵$扬州大学物理科学与技术学院!江苏扬州,225002~~~~~~~~     

介孔分子筛SBA-15负载的双亚胺镍催化剂的合成及乙烯聚合

应用新型介孔分子筛SBA-15为载体, 成功地对后过渡金属镍双亚胺催化剂进行了物理和化学负载, 并应用元素分析, 等离子体发射光谱(ICP), FT-IR和X射线粉末衍射(XRD)等对载体催化剂进行了表征. 乙烯聚合结果表明, 载体催化剂不仅具有镍双亚胺均相催化剂的高活性, 而且由于载体孔道效应生成了纤维状聚乙烯, 同时聚合物的分子量和分子量分布较均相催化剂有大幅度提高.     

Studies on syntheses of biscrown ether compounds

Multi-ester type biscrown ether compound(I) was prepared by the reaction of 6-bromoacetacetic ester dibenzo-16-crown-5(7) with phenyl-methyl ether-2,6-diformic acid potassium salt in anhydrous DMF at refluxed temperature, and color biscrown ether compound(II) was prepared by the reaction of 4′-aminobenzo-15-crown-5(12) with 2,2′(O-formoyl naphthyl)ethyl ether (9) in anhydrous ethanol at 40 C under N₂. New compounds(I, II) were characterized by IR,¹H NMR, MS and elemental analysis. Supported by the National Natural Science Foundation of China Niu Changrong: born in December, 12, 1938, Professor     

Atomic-scale computer simulation for early precipitation process of Ni75Al10V15 alloy

The kinetic model for a ternary system is introduced based on the microscopic diffusion form of the phase-field equations for a binary alloy. The equation is solved in the reciprocal space. This model is used to investigate the early precipitation process of Ni75-Al10V15 by simulating the atomic pictures of the two ordered phases and calculating the order parameters of γ′(Ni3Al) phase. Simulation results show that the γ′ ordered phases precipitate from the disordered matrix by a non-classical nucleation mechanism, and the nonstoichiometric γ′ ordered phase appears first and then transforms into the stoichiometric one. Clusters of V atoms appear at the γ′ phase boundaries followed by the formation of the nonstoichiometric θ ordered phase. The farther the location from γ′ phase boundary is, the lower the order degree of θ phase is. There exist two kinds of DO22 ordered domains: a horizontal one and a vertical one, related to their adjacent γ′ phase boundaries. The model could describe the atomic ordering and composition clustering simultaneously, and any a priori assumption about the new phase structure and precipitation mechanism etc. is unnecessary.     

掺Pr3+钛酸盐红色长余辉发光性质比较

通过荧光光谱和磷光衰减曲线比较了CaTiO3∶Pr3+(CaTP),Ca0.8Zn0.2TiO3∶Pr3+ (CaZnTP)和Ca2Zn4Ti15O36Pr3+(Ca2Zn4TP)掺Pr3+钛酸盐的红色长余辉发光性质.测定了它们的热释光曲线.CaTP,CaZnTP和Ca2Zn4TP的热释光峰值分别是49 ℃,62 ℃和75 ℃,热释峰相对强度分别是220,186和1 254,这表明掺Pr3+钛酸盐晶体中的缺陷陷阱能级深度为Ca2Zn4TP>CaZnTP>CaTP,陷阱中电子的逸出速率是CaZnTP>CTP>Ca2Zn4TP.从理论上解释了余辉时间顺序为Ca2Zn4TP > CaZnTP > CaTP,起始发光强度顺序为CaZnTP>CTP>Ca2Zn4TP的变化规律.     

我国U15男子篮球运动员“手感”与“步法”技术能力的发展现状及成因

为探究我国U15男子篮球运动员的"手感"与"步法"技术能力的发展现状,运用文献资料、数理统计、测试和访谈等研究方法,对2012~2016年参加全国U15男子篮球比赛运动员的专项技术成绩数据进行整理和解析,并依照时间顺序对各批次运动员完成各项技术的状况进行纵向动态比较,且对成因进行深入剖析.据此,对我国青少年篮球运动员在专项技术能力培养方面提出加强考核内容及标准的灵活性和注重训练内容的均衡性等建议,力求为我国男子篮球竞技后备人才的可持续性发展提供有益参考.     

我国U-15足球队群体凝聚力水平现状分析

应用"群体环境问卷"对我国U-15足球队凝聚力水平进行全面的调查研究,分析影响我国U-15足球队凝聚力的多种因素.研究结果表明,我国U-15足球队凝聚力总体水平普遍偏低,任务凝聚力水平高于交往凝聚力水平;不同训练年限的运动员任务凝聚力水平具有显著性差异;不同司职位置间运动员任务凝聚力水平存在显著性差异;主力、替运动员间交往凝聚力水平存在显著性差异;不同运动等级运动员间任务凝聚力水平存在显著性差异.     

东兴煤业15号煤层的采区布置及装备选型

在对东兴煤业地质条件、煤层储存条件分析的基础上，就15号煤层的采煤方法、工作面顶板管理方式、支护设备选型、回采工作面的长度、采高和巷道布置进行了研究。研究结果表明：放顶煤综采工艺适合本矿现有的生产条件，工作面顶板管理简单易行。     

砂轮粒度及其修整影响GCr15钢磨削表面质量的研究

本文探讨了砂轮粒度及其修整对滚动轴承钢Gcr15磨削表面质量的影响。采用不同粒度、不同修整导程的砂轮分别在外圆磨床上进行切入式横磨,对磨削力、磨削温度、工件表层显微硬度及其表面粗糙度等影响均作了试验研究。结果表明,合理选择砂轮粒度与修整导程是提高滚动轴承钢磨削表面质量的重要途径之一。